1. 鎳-鎢-鈷合金電刷鍍液的性質


  鎳-鎢-鈷合金電刷鍍液是在鎳-鎢合金鍍液的基礎上加入少量的硫酸鈷等成分組成的鎳-鎢-鈷鍍液。它是酸性鍍液,pH=1.2~2.4,深綠色,20℃時相對密度為1.29,電導率為2.052 Ω-1·cm-1



2. 鎳-鎢-鈷合金電刷鍍層的性質和(he)用途


  鎳(nie)-鎢-鈷鍍層(ceng)硬度(du)(du)高(gao),致密(mi)、孔隙(xi)少(shao),在較(jiao)高(gao)的溫度(du)(du)下(xia)仍具有一定的硬度(du)(du),其優(you)點是鍍層(ceng)的應力小,可(ke)沉積較(jiao)厚的鍍層(ceng),即可(ke)達0.20mm,主要用來沉積耐磨的表面層(ceng)。



3. 鎳(nie)-鎢-鈷合金(jin)電刷鍍液的(de)成分(fen)


 硫酸鎳(NiSO4·7H2O)   393g/L  、 硫酸鎂(MgSO4·7H2O)  2g/L


 鎢酸鈉(Na2WO4·2H2O)   23g/L  、冰醋酸(CH3COOH)  20mL/L


 甲酸(HCOOH)  35g/L  、 硼酸(H3BO3) 31mL/L  、氟化鈉(NaF) 5g/L


 檸檬酸(H3C6H5O7·H2O)  42g/L  、硫酸鈉(Na2SO4)  6.5g/L


 十二烷基硫酸鈉[CH3(CH2)11 SO4Na]  0.01~0.001g/L


 硫酸鈷(CoSO4·7H2O)  2g/L   、 硫酸錳(MnSO4·4H2O)  2g/L



4. 鎳-鎢-鈷合金電刷鍍(du)液的配制


  在1000mL燒(shao)(shao)杯(bei)(bei)中(zhong)(zhong)(zhong)加(jia)(jia)(jia)(jia)入(ru)(ru)(ru)蒸(zheng)(zheng)餾(liu)(liu)水350mL,加(jia)(jia)(jia)(jia)熱(re)(re)(re)至(zhi)(zhi)70℃,加(jia)(jia)(jia)(jia)入(ru)(ru)(ru)硫(liu)(liu)(liu)酸(suan)(suan)(suan)(suan)鎳393g,攪(jiao)(jiao)(jiao)(jiao)(jiao)拌(ban)(ban)溶(rong)(rong)解。另(ling)(ling)取(qu)250ml,燒(shao)(shao)杯(bei)(bei),加(jia)(jia)(jia)(jia)水100ml,加(jia)(jia)(jia)(jia)熱(re)(re)(re)至(zhi)(zhi)70℃,加(jia)(jia)(jia)(jia)入(ru)(ru)(ru)檸檬酸(suan)(suan)(suan)(suan)42g,攪(jiao)(jiao)(jiao)(jiao)(jiao)排溶(rong)(rong)解后(hou),加(jia)(jia)(jia)(jia)入(ru)(ru)(ru)鴨酸(suan)(suan)(suan)(suan)鈉(na)(na)23,加(jia)(jia)(jia)(jia)熱(re)(re)(re)攪(jiao)(jiao)(jiao)(jiao)(jiao)拌(ban)(ban)館解后(hou),加(jia)(jia)(jia)(jia)入(ru)(ru)(ru)含硫(liu)(liu)(liu)酸(suan)(suan)(suan)(suan)鎳的溶(rong)(rong)液(ye)中(zhong)(zhong)(zhong),攪(jiao)(jiao)(jiao)(jiao)(jiao)拌(ban)(ban)均勻。另(ling)(ling)取(qu)在250mL燒(shao)(shao)杯(bei)(bei)中(zhong)(zhong)(zhong)加(jia)(jia)(jia)(jia)入(ru)(ru)(ru)蒸(zheng)(zheng)餾(liu)(liu)水100ml,加(jia)(jia)(jia)(jia)熱(re)(re)(re)至(zhi)(zhi)70℃,加(jia)(jia)(jia)(jia)入(ru)(ru)(ru)硼酸(suan)(suan)(suan)(suan)31g,加(jia)(jia)(jia)(jia)熱(re)(re)(re)攪(jiao)(jiao)(jiao)(jiao)(jiao)拌(ban)(ban)溶(rong)(rong)解后(hou),加(jia)(jia)(jia)(jia)入(ru)(ru)(ru)含硫(liu)(liu)(liu)酸(suan)(suan)(suan)(suan)鎳的溶(rong)(rong)液(ye)中(zhong)(zhong)(zhong),攪(jiao)(jiao)(jiao)(jiao)(jiao)拌(ban)(ban)均勻。另(ling)(ling)取(qu)在250mL燒(shao)(shao)杯(bei)(bei)中(zhong)(zhong)(zhong)加(jia)(jia)(jia)(jia)蒸(zheng)(zheng)餾(liu)(liu)水50ml,加(jia)(jia)(jia)(jia)熱(re)(re)(re)至(zhi)(zhi)70℃,加(jia)(jia)(jia)(jia)入(ru)(ru)(ru)硫(liu)(liu)(liu)酸(suan)(suan)(suan)(suan)鈉(na)(na)6.5g、硫(liu)(liu)(liu)酸(suan)(suan)(suan)(suan)鈷2g、硫(liu)(liu)(liu)酸(suan)(suan)(suan)(suan)錳28、硫(liu)(liu)(liu)酸(suan)(suan)(suan)(suan)鎂2g和(he)氟化(hua)鈉(na)(na)5g,加(jia)(jia)(jia)(jia)熱(re)(re)(re)攪(jiao)(jiao)(jiao)(jiao)(jiao)拌(ban)(ban)溶(rong)(rong)解后(hou),加(jia)(jia)(jia)(jia)人含硫(liu)(liu)(liu)酸(suan)(suan)(suan)(suan)鎳的溶(rong)(rong)液(ye)中(zhong)(zhong)(zhong),攪(jiao)(jiao)(jiao)(jiao)(jiao)拌(ban)(ban)均勻。另(ling)(ling)加(jia)(jia)(jia)(jia)十二烷(wan)基(ji)硫(liu)(liu)(liu)酸(suan)(suan)(suan)(suan)鈉(na)(na)0.01~0.001g充分攪(jiao)(jiao)(jiao)(jiao)(jiao)拌(ban)(ban)溶(rong)(rong)解。再加(jia)(jia)(jia)(jia)人甲酸(suan)(suan)(suan)(suan)35mL 和(he)冰醋(cu)酸(suan)(suan)(suan)(suan)20mL,加(jia)(jia)(jia)(jia)熱(re)(re)(re)充分攪(jiao)(jiao)(jiao)(jiao)(jiao)拌(ban)(ban)至(zhi)(zhi)溶(rong)(rong)液(ye)透明(ming)。冷卻至(zhi)(zhi)室(shi)溫(wen),用10%稀硫(liu)(liu)(liu)酸(suan)(suan)(suan)(suan)或(huo)稀氫氧化(hua)鈉(na)(na)溶(rong)(rong)液(ye)調節溶(rong)(rong)液(ye)pH為2.將(jiang)溶(rong)(rong)液(ye)倒入(ru)(ru)(ru)1000mL量筒或(huo)量瓶中(zhong)(zhong)(zhong),加(jia)(jia)(jia)(jia)蒸(zheng)(zheng)餾(liu)(liu)水至(zhi)(zhi)刻度。



5. 鎳-鎢-鈷(gu)合金鍍液工藝規范(fan)


 鎳(nie)-鎢-鈷合金(jin)鍍液性能上比(bi)較類(lei)似于(yu)鎳(nie)-鎢合金(jin)鍍液。


 耗(hao)電系數:0.21A·h/(d㎡·μm);


 工作電(dian)壓(ya):6~12V(最佳(jia)10~12V);


 陰陽極相(xiang)對運(yun)動速率:6~12m/min;


 工作溫度:30~50℃.


 循環使用過程可參(can)照鎳-鎢合金(jin)刷鍍液。